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Instrumentation in Gel Chromatography

  • A standard gel chromatography system typically includes:

Instrumentation in Gel Chromatography

Pump:

  • Delivers a steady flow of the mobile phase (often a buffered aqueous solution).

Sample Injector:

  • Introduces the sample into the mobile phase. Automated injectors provide reproducibility and accuracy.

Column:

  • Packed with porous beads made from agarose, dextran, polyacrylamide, or polystyrene. Column size and pore characteristics are chosen based on the target separation.

Detectors:

  • Refractive Index Detector: Common for detecting carbohydrates and general solutes.

  • UV Detector: Ideal for biomolecules (proteins, nucleic acids) absorbing at specific UV wavelengths.

  • Light Scattering Detector: Enables direct determination of molar mass.

Temperature Control Unit:

  • Maintains stable temperature conditions to preserve sample integrity or improve resolution.

Data System (Recorder/Software):

  • Modern chromatography systems interface with computers for real-time data acquisition, peak integration, and molecular weight determination.


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