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Methods of Preparation of Ophthalmic


Aseptic Filtration

  • The formulation (solution) is passed through a sterile 0.22 μm membrane filter, removing bacteria and other particulates.

  • The filtered solution is then filled into previously sterilized containers under laminar airflow conditions.

Terminal Sterilization

  • If the formulation and container can withstand heat, autoclaving at 121°C for 15–20 minutes is often employed.

  • Advantages: higher sterility assurance level.

  • Disadvantages: not suitable for heat-labile drugs.

Dry Heat Sterilization (for Ointments)

  • The base can be sterilized by heating in an oven at 160–170°C for a specific time.

  • Drug powders might be sterilized separately if stable to heat, then mixed under aseptic conditions.

Gamma Irradiation or Ethylene Oxide

  • Used in specialized cases (e.g., certain packaging materials).

  • Less common for routine ophthalmic solutions due to potential effects on drug stability and safety.


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