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pH Determination

  • Accurate pH measurement is essential in laboratories, industry, and research.

pH Determination

Electrometric Methods

Principle:

  • Based on the measurement of the electromotive force (EMF) of a galvanic cell that includes a pH-sensitive electrode.

Components:

  • Glass Electrode: Sensitive to hydrogen ion activity; develops a potential proportional to pH.

  • Reference Electrode: Provides a constant potential; commonly a silver/silver chloride or calomel electrode.

  • pH Meter: Reads the potential difference and displays the pH.

Procedure:

  • Calibrate the pH meter using standard buffer solutions of known pH.

  • Rinse electrodes with distilled water.

  • Immerse electrodes in the test solution.

  • Record the stable pH reading.

Advantages:

  • High accuracy and precision.

  • Suitable for a wide pH range.

  • Can measure pH in colored or turbid solutions.

Applications:

  • Research laboratories.

  • Quality control in manufacturing.

  • Clinical diagnostics.

Colorimetric Methods

Principle:

  • Utilize pH indicators that change color depending on the pH of the solution.

Indicators:

  • Weak acids or bases with different colors in protonated and deprotonated forms.

  • Common indicators include litmus, phenolphthalein, methyl orange, and bromothymol blue.

Procedure:

  • Add a few drops of indicator to the test solution.

  • Observe the color change.

  • Compare the color to a standard pH color chart.

Advantages:

  • Simple and cost-effective.

  • Quick estimation of pH.

Limitations:

  • Less precise than electrometric methods.

  • Subjective interpretation of color.

  • Not suitable for colored or opaque solutions.

Applications:

  • Educational demonstrations.

  • Field testing where equipment is unavailable.


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